Reaction Tips & Tricks for Organic Syntheses
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Reaction Tips & Tricks for Organic Syntheses
Detailed Information for Carrying out Chemical Synthesis Reactions
Tips.reactiontips.com news digest
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9 years
Invented by Professor Oyo Mitsunobu in 1967
Here is a video explaining the Mechanism of Mitsunobu Reaction!
Recently DEAD has been replaced with less harmful DIAD -
10 years
Scalable Solvent free sillylation of alcohols
Procedure
Charged 100g of staring alcohol (liquid or solid) to a 1L 4 neck RBF under nitogen atmosphere.
Added 2.5 Meq. of imidazole at RT. -
11 years
Esterification of a diversly functionalized molecule
One of our colleagues has to perform an esterfication reaction to prepare ester derivative of a carboxylic acid function bearing compound. The compound has a secondary OH and N-Ac functions in addition to the carboxyl group. Use of oxalyl chloride was...
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12 years
Acetonide protection in presence of acid sensitive O-Protection
Acetonide protection in presence of acid sensitive O-protective group is very critical. You have to be very careful during this reaction. Usually acetonide protection has been carried out in presence of catalytic amount of p-TSA in acetone.
But when you have acid sensitive protective group such as TBDMS, TBDPS etc, donot use p-TSA more than 0.001 equivalent otherwise acid sensitive protective group does not stand any more. The best procedure is the use of 2,2'-dimethoxy propane with 0....
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